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File Name: Diisobutylaluminium_hydride_1.0M_in_toluene.asp

                              SIGMA-ALDRICH

Material Safety Data Sheet

Date Printed: 28/JUN/2005
Date Updated: 10/FEB/2005
Version 1.2
According to 91/155/EEC

Classified as Hazardous according to the criteria of EU Annex 1 and
NOHSC.

1 - Product and Company Information

Product Name DIISOBUTYLALUMINUM HYDRIDE, 1.0M
SOLUTION IN TOLUENE
Product Number 256870

Company Sigma-Aldrich Pty. Ltd.
12 Anella Avenue
Castle Hill NSW 2154
Australia
Technical Phone # +61 2 9841 0555 (1800 800 097)
Fax +61 2 9841 0500 (1800 800 096)
Emergency Phone # +44 8701906777 (1800 448 465)

2 - Composition/Information on Ingredients

Product Name CAS # EC no Annex I
Index Number
DIISOBUTYLALUMINUM HYDRIDE,1.0M None None None
SOLUTION IN TOLUENE

Formula C8H19Al
Molecular Weight 142.22 AMU

3 - Hazards Identification

SPECIAL INDICATION OF HAZARDS TO HUMANS AND THE ENVIRONMENT
Highly flammable. Reacts violently with water, liberating
extremely flammable gases. Toxic by inhalation, in contact with
skin and if swallowed. Causes burns.


4 - First Aid Measures

AFTER INHALATION
If inhaled, remove to fresh air. If not breathing give
artificial respiration. If breathing is difficult, give oxygen.

AFTER EYE CONTACT
Assure adequate flushing of the eyes by separating the eyelids
with fingers.

AFTER INGESTION
If swallowed, wash out mouth with water provided person is
conscious. Call a physician.

5 - Fire Fighting Measures

CONDITIONS OF FLAMMABILITY
Catches fire if exposed to air. Reacts with water to liberate
flammable and/or explosive gas.

EXTINGUISHING MEDIA
Suitable: Dry chemical powder.
Unsuitable: Do not use water.
Explosion Hazards: Container explosion may occur under fire
conditions.

SPECIAL PROTECTIVE EQUIPMENT FOR FIREFIGHTERS
Wear self-contained breathing apparatus and protective clothing
to prevent contact with skin and eyes.

6 - Accidental Release Measures

PERSONAL PRECAUTION PROCEDURES TO BE FOLLOWED IN CASE OF LEAK OR SPILL
Evacuate area. Shut off all sources of ignition.

METHODS FOR CLEANING UP
Cover with dry-lime, sand, or soda ash. Place in covered
containers using non-sparking tools and transport outdoors.
Ventilate area and wash spill site after material pickup is
complete.

7 - Handling and Storage

HANDLING
Directions for Safe Handling: Do not breathe vapor. Do not get
in eyes, on skin, on clothing. Avoid prolonged or repeated
exposure.

STORAGE
Conditions of Storage: Keep tightly closed. Keep away from
combustible materials, heat, sparks, and open flame. Store in a
cool dry place.
Incompatible Materials: Do not allow contact with water

SPECIAL REQUIREMENTS: May develop pressure. Open carefully. Air
sensitive. Handle and store under inert gas.

8 - Exposure Controls / Personal Protection

ENGINEERING CONTROLS
Use only in a chemical fume hood. Safety shower and eye bath.

GENERAL HYGIENE MEASURES
Remove and wash contaminated clothing promptly. Wash thoroughly
after handling.

PERSONAL PROTECTIVE EQUIPMENT
Special Protective Measures: Wear appropriate government approved
respirator, chemical-resistant gloves, safety goggles, other
protective clothing. Faceshield (8-inch minimum).

9 - Physical and Chemical Properties

Appearance N/A

Property Value At Temperature or Pressure

pH N/A
BP/BP Range N/A
MP/MP Range N/A


ALDRICH - 256870 www.sigma-aldrich.com Page 2
Flash Point 4 掳C Method: closed cup
Flammability N/A
Autoignition Temp N/A
Oxidizing Properties N/A
Explosive Properties N/A
Explosion Limits N/A
Vapor Pressure N/A
SG/Density 0.858 g/cm3
Partition Coefficient N/A
Viscosity N/A
Vapor Density N/A
Saturated Vapor Conc. N/A
Evaporation Rate N/A
Bulk Density N/A
Decomposition Temp. N/A
Solvent Content N/A
Water Content N/A
Surface Tension N/A
Conductivity N/A
Miscellaneous Data N/A
Solubility N/A

10 - Stability and Reactivity

STABILITY
Reactions to Avoid: Reacts violently with:
Materials to Avoid: Alcohols, Water, Oxygen, Oxidizing agents.

HAZARDOUS DECOMPOSITION PRODUCTS
Hazardous Decomposition Products: Carbon monoxide, Carbon dioxide,
Aluminum oxide, Liberates flammable/explosive hydrogen gas.

11 - Toxicological Information

SIGNS AND SYMPTOMS OF EXPOSURE
Inhalation studies on toluene have demonstrated the development
of inflammatory and ulcerous lesions of the penis, prepuce, and
scrotum in animals. Exposure can cause: Nausea, headache, and
vomiting.

ROUTE OF EXPOSURE
Multiple Routes: Harmful if swallowed, inhaled, or absorbed
through skin. Causes burns. High concentrations are extremely
destructive to tissues of the mucous membranes and upper
respiratory tract, eyes, and skin.

TARGET ORGAN INFORMATION
Brain. Liver. Kidneys. Bladder.

CONDITIONS AGGRAVATED BY EXPOSURE
May cause nervous system disturbances.

12 - Ecological Information

No data available.

13 - Disposal Considerations

SUBSTANCE DISPOSAL
Under an inert atmosphere, cautiously add the material to dry
butanol in an appropriate solvent. The chemical reaction may be
vigorous and/or exothermic. Provisions must be made for the


ALDRICH - 256870 www.sigma-aldrich.com Page 3
venting of large volumes of highly flammable hydrogen and/or
hydrocarbon gases. Neutralize the solution with aqueous acid.
Filter off any solid residues for disposal as hazardous waste.
Burn the liquid portion in a chemical incinerator equipped with an
afterburner and scrubber. Observe all federal, state, and local
environmental regulations.

14 - Transport Information

RID/ADR
UN#: 3399
Class: 4.3
PG: I
Proper Shipping Name: Organometallic substance,
liquid, water-reactive, flammable

IMDG
UN#: 3399
Class: 4.3
PG: I
Subrisk: 3
Proper Shipping Name: Organometallic substance,
liquid, water-reactive, flammable
Marine Pollutant: No
Severe Marine Pollutant: No
Technical Name: Required

IATA
UN#: 3399
Class: 4.3
PG: I
Subrisk: 3
Proper Shipping Name: Organometallic substance,
liquid, water-reactive, flammable
Inhalation Packing Group I: No
Technical Name: Required

15 - Regulatory Information

CLASSIFICATION AND LABELING ACCORDING TO EU DIRECTIVES
INDICATION OF DANGER: F T
Highly Flammable. Toxic.
R-PHRASES: 11 14/15 23/24/25 34
Highly flammable. Reacts violently with water, liberating
extremely flammable gases. Toxic by inhalation, in contact with
skin and if swallowed. Causes burns.
S-PHRASES: 16 26 36/37/39 45
Keep away from sources of ignition - no smoking. In case of
contact with eyes, rinse immediately with plenty of water and
seek medical advice. Wear suitable protective clothing, gloves,
and eye/face protection. In case of accident or if you feel
unwell, seek medical advice immediately (show the label where
possible).

16 - Other Information

WARRANTY
The above information is believed to be correct but does not
purport to be all inclusive and shall be used only as a guide. The
information in this document is based on the present state of our
knowledge and is applicable to the product with regard to
appropriate safety precautions. It does not represent any


ALDRICH - 256870 www.sigma-aldrich.com Page 4
guarantee of the properties of the product. Sigma-Aldrich Inc.,
shall not be held liable for any damage resulting from handling or
from contact with the above product. See reverse side of invoice
or packing slip for additional terms and conditions of sale.
Copyright 2005 Sigma-Aldrich Co. License granted to make unlimited
paper copies for internal use only.

DISCLAIMER
For R&D use only. Not for drug, household or other uses.




ALDRICH - 256870 www.sigma-aldrich.com Page 5

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