Material Safety Data Sheet
Reviewed 5/03
Section I
Manufacturer's Name Non-Emergency Telephone #
Coatings For Industry, Inc. 215-723-0919
Address Emergency Telephone #
319 Township Line Road 1-800-535-5053
Souderton, PA 18964
Chemical Name & Synonyms Chemical Family
1,6 Hexamethylene Diisocyanate Aliphatic Isocyanate
Based Polyisocyanate
Trade Name & Synonyms
Urethabond 111 Part B,
Urethabond 145 Part B,
Urethabond 150 Part B,
Urethabond 166 Part B,
Urethabond 169 Part B,
Urethabond 313 Part B,
Urethabond 350 Part B
Boostercoat Type 1
Mod. B
NB#387026
Section II - Hazardous Ingredients
% TLV CAS #
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Homopolymer of HDI
75% OSHA: Not Established 28182-81-2
ACGIH: Not Established
The manufacturer recommended guideline level for exposure to HDI based
polyisocyanates is:
0.5 mg/m3 TWA over 8 hours &
1.0 mg/m3 stel over 15 minutes
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Hexamethylene
Diisocyanate (HDI) * OSHA: Not Established 822-06-0
ACGIH:.005 ppm TWA
*Residual monomer content less than 0.5% based on resin solids at the time of manufacture.
However, after 3-6 months storage, the free monomer content may rise to a maximum of 1.6%.
Manufacturer recommends a ceiling level of 0.02 ppm.
U-111 Part B Page 2 of 10
Section II - Hazardous Ingredients (cont.)
% TLV CAS #
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Xylene 12.5% OSHA: 100 ppm TWA 1330-20-7
150 ppm stel
ACGIH:100 ppm TWA
150 ppm stel
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N Butyl Acetate 12.5% OSHA: 150 ppm TWA 123-86-4
200 ppm stel
ACGIH:150 ppm TWA
200 ppm stel
This document is prepared pursuant to the OSHA Hazard Communication Standard (29 CFR
1910.1200). In addition, other substances not "hazardous" per this OSHA standard may be
listed.
Section III - Physical Data
Specific Gravity ~~~~~~~~~~~~~~~1.06 @ 68?F. (20?C.)
% Volatile by Volume ~~~~~~~~~~ Approximately 30%
Bulk Density ~~~~~~~~~~~~~~~~~ 8.85 lb./gallon
Vapor Pressure ~~~~~~~~~~~~~~~ Polyisocyanate: Approx. 7.5 x 10-5 mm hg
@ 20?C.
Butyl Acetate: 15 mm hg @ 25?C.
Xylene: 9 mm hg @ 20?C.
Molecular Weight ~~~~~~~~~~~~~~ Approx. 500 (Polyisocyanate)
Water Solubility ~~~~~~~~~~~~~~~~ Resin is insoluble - reacts slowly with
water to liberate CO2 gas
Appearance & Odor ~~~~~~~~~~~~~ Clear/pale yellow liquid with solvent odor
Section IV - Fire and Explosion Data
Flash point ~~~~~~~~~~~~~~~~~~~ 91.0?F. (32.7?C.) Setaflash
Flammable Limits:
UEL: 7.0 Xylene
7.6 N-Butyl Acetate
LEL: 1.0 Xylene
1.38 N-Butyl Acetate
Extinguishing Media ~~~~~~~~~~~~Dry chemical; carbon dioxide; foam; water spray for large
fires.
Special Fire Fighting Procedures:
Full emergency equipment with self contained breathing apparatus and full protective clothing
should be worn by fire fighters. During a fire, HDI vapors and other irritating, highly toxic gases
may be generated by thermal decomposition or combustion. (see Section VIII).
Isolate from heat, electrical equipment, sparks and open flame. Closed container may explode
when exposed to extreme heat or burst when contaminated with water (CO2 evolved).
Solvent vapors may be heavier than air. Stagnant air may cause vapors to accumulate and travel
along the ground to an ignition source which may result in a flash back to the source of the
vapors.
U-111 Part B Page 3 of 10
Section V - Human Health Data
Route of entry ~~~~~~~~~~~~~~~~ Inhalation; skin contact; eye contact.
Human Effects and Symptoms of Overexposure:
Acute Inhalation: HDI vapors or mist at concentrations above the TLV or MGL can irritate
(burning sensation) the mucous membranes in the respiratory tract (nose, throat, lungs) causing
runny nose, sore throat, coughing, chest discomfort, shortness of breath and reduced lung
function (breathing obstruction).
Persons with a preexisting, nonspecific bronchial hyperreactivity can respond to concentrations
below the TLV or the manufacturer's suggested guideline with similar symptoms as well as an
asthma attack. Exposure well above the TLV or manufacturer's suggested guildeline may lead to
bronchitis, bronchial spasm and pulmonary edema (fluid in lungs). These effects are usually
reversible. Chemical or hypersensitive pneumonitis, with flu-like symptoms (e.g., fever, chills)
has also been reported.
Solvent vapors may be irritating to the eyes, nose and throat. Symptoms of irritation may
include: redness, burning, and itching of the eyes, dryness of the throat and tightness of the chest.
Other possible symptoms of overexposure include: headache, nausea, narcosis, fatigue and loss
of appetite.
A concentration of 200 ppm Butyl Acetate can cause eye, nose, and throat irritation. At 300 ppm
these effects can become severe. Persons exposed to 200 ppm of xylene experienced eye, nose
and throat irritation. Concentrations of 10,000 ppm of Xylene can be immediately dangerous to
life and health.
Chronic Inhalation: As a result of previous repeated overexposures or a single large dose,
certain individuals will develop isocyanate sensitization (chemical asthma) which will cause
them to react to a later exposure to isocyanate at levels well below the TLV or manufacturer's
suggested guideline.
These symptoms, which include: chest tightness, wheezing, cough, shortness of breath or
asthmatic attack, could be immediate or delayed up to several hours after exposure. Similar to
many non-specific asthmatic responses, there are reports that once sensitized an individual can
experience these symptoms upon exposure to dust, cold air or other irritants. This increased lung
sensitivity can persist for weeks and in severe cases for several years.
Chronic overexposure to isocyanate has also been reported to cause lung damage, including
decrease in lung function, which may be permanent. Sensitization may be either temporary or
permanent. Chronic exposure to organic solvents has been associated with various neurotoxic
effects including permanent brain and nervous system damage. Symptoms include: loss of
memory, loss of intellectual ability and loss of coordination.
Acute Skin Contact: Isocyanates react with skin protein and moisture and can cause irritation.
Symptoms of skin irritation may be reddening, swelling, rash, scaling or blistering. Some
persons may develop skin sensitization from skin contact. Cured material is difficult to remove.
Repeated or prolonged skin contact with solvents can result in dry, defatted and cracked skin
causing increased susceptibility to infection. In addition, skin irritation (i.e. redness, swelling),
which may develop into dermatitis, may occur from skin contact. Solvents can penetrate the skin
and may cause systemic effects similar to those identified under acute inhalation symptoms.
Chronic Skin Contact: Prolonged contact with the isocyanate can cause reddening, swelling,
rash, scaling or blistering. In those who have developed a skin sensitization, these symptoms can
develop as a result of contact with very small amounts of liquid material or even as a result of
vapor only exposure. Chronic skin exposure to solvents may cause effects similar to those
identified under chronic inhalation effects.
Acute Eye Contact: Liquid, aerosols and vapors of this product (isocyanate and solvents) are
irritating and can cause tearing, reddening and swelling accompanied by a stinging sensation
and/or feeling like that of fine dust in the eyes.
U-111 Part B Page 4 of 10
Human Effects and Symptoms of Overexposure (cont.)
Chronic Eye Contact: May result in corneal opacity (clouding of the eye surface). Prolonged
vapor contact may cause conjunctivitis.
Acute Ingestion: Can result in irritation and possible corrosive action in the mouth, stomach
tissue and digestive tract. Vomiting may cause aspiration of the solvent resulting in chemical
pneumonitis.
Chronic Ingestion: None found
Carcinogenicity
NTP ~~~~~~~~~~~~~~~~~ Not Listed
IARC ~~~~~~~~~~~~~~~~ Not Listed
OSHA ~~~~~~~~~~~~~~~~Not Regulated
Medical Conditions Aggravated by Exposure: Asthma and other respiratory disorders
(bronchitis, emphysema, hyperreactivity), skin allergies, eczema.
Exposure Limits: Not established for product as a whole. Refer to Section II for exposure
limits of hazardous constituents. The manufacturer suggested guidelines of 0.5 mg/m3 TWA
and 1.0 mg/m3 stel for the homopolymer of HDI and 0.02 ppm ceiling for HDI monomer are
guides based on limited data; provided pending the review of future data.
Section VI - Emergency and First Aid Procedures
First Aid for Eyes:
Flush with clean, lukewarm water (low pressure) for at least 15 minutes, while lifting eyelids.
Refer individual to physician or ophthalmologist for immediate follow up.
First Aid for Skin:
Remove contaminated clothing immediately. Wash affected areas thoroughly with soap and
water. Wash contaminated clothing thoroughly before reuse. For severe exposures, get under
safety shower after removing clothing, then get medical attention. For lesser exposures, seek
medical attention if irritation develops or persists.
First Aid for Inhalation:
Move to an area free from risk of further exposure. Administer oxygen or artificial respiration as
needed. Obtain medical attention. Asthmatic type symptoms may develop and may be
immediate or delayed up to several hours. Treatment is essentially symptomatic. Consult
physician.
First Aid for Ingestion:
Do not induce vomiting. Give 1 to 2 cups of milk or water to drink. Do not give anything by
mouth to an unconscious or convulsing person. Consult physician.
Note to Physician.........
Eyes: Stain for evidence of corneal injury. If cornea is burned, instill antibiotic/steriod
preparation frequently. Workplace vapors could produce reversible corneal epithelial edema
impairing vision.
Skin: This product is a known skin sensitizer. Treat symptomatically as for contact dermatitis
or thermal burn.
Ingestion: Treat symptomatically. There is no specific antidote. Inducing vomiting is
contraindicated because of the irritating nature of the product.
U-111 Part B Page 5 of 10
Inhalation: This product is a known pulmonary sensitizer. Treatment is essentially
symptomatic. An individual having a dermal or pulmonary sensitization reaction to this material
must be removed from any further exposure to any isocyanate.
Section VII - Employee Protection Recommendations
Required work/hygiene procedures:
Precautions must be taken so that persons handling product do not breathe the vapors or have it
contact the eyes or skin. In spray operations, protection must be afforded against exposure to
both vapor and spray mist.
Eye protection requirements:
Safety glasses, splash goggles or face shield. Contact lenses should not be worn.
Skin protection requirements:
Permeation resistant gloves. Cover as much of the exposed skin area as possible with
appropriate clothing. If skin creams are used, keep the area protected only by the cream to a
minimum.
Respirator requirements:
A respirator that is recommended or approved for use in isocyanate containing environments
(air purifying or fresh air supplied) may be necessary. Consider type of application and
environmental concentrations. Observe OSHA regulations for respirator use (29CFR1910.134).
Note on Odor Warning Properties: Pure isocyanate materials have odor thresholds that are
higher than the TLV, PEL or manufacturer's suggested guidelines. Thus, if a vapor/particulate
air-purifying respirator has exceeded its service life, breakthrough of the filter can result in
exposure over the allowable limit without the wearer being able to smell the isocyanate.
However, when a polyurethane coating system contains organic solvents, the wearer of a vapor
particulate respirator will be warned of filter breakthrough by the odor of solvents before being
exposed to isocyanates because:
1) Organic solvents have low odor thresholds.
2) Testing has demonstrated that solvents break through filters before isocyanates do.
Spray Application:
Good industrial hygiene practice dictates that when isocyanate based coatings are spray applied,
some form of respiratory protection should be worn. During the spray application of organic
solvent containing coatings systems, the use of a positive pressure supplied air respirator is
mandatory when:
~ the airborne isocyanate concentrations are not known, or
~ the airborne HDI monomer concentrations exceed 0.05 ppm (10 times the TLV) or the
polyisocyanate (polymeric, oligomeric) concentrations exceed 5 mg/m3 averaged over 8 hours or
10 mg/m3 averaged over 15 minutes (10 times the manufacturer's suggested guideline) or
~ spraying is performed in a confined space or in an area with limited ventilation.
A properly fitted air purifying (combination organic vapor and particulate) respirator, proven by
test to be effective in isocyanate-containing spray paint environments, will provide adequate
protection when:
~ the airborne HDI monomer concentrations is known to be below 0.05 ppm (10 times the TLV)
~ the polyisocyanate (polymeric, oligomeric) concentrations are known to be below 5 mg/m3
averaged over 8 hours or 10 mg/m3 averaged over 15 minutes (10 times the manufacturer's
suggested guideline).
U-111 Part B Page 6 of 10
Non-spray Operations:
Even during non-spray operations such as mixing, batch making, brush or roller application, etc.,
depending on the conditions (for example, heating of material or application to a hot substrate),
it is possible to be exposed to airborne isocyanate vapors. Therefore, when the coatings system
contains solvents and will be applied in a non-spray manner, a positive pressure supplied air
respirator must be worn when:
~ the airborne concentrations are unknown; or
~ the airborne HDI monomer concentrations exceed 0.05 ppm (10 times the TLV), or
~ the airborne concentrations of the polyisocyanate (polymeric, oligomeric) exceed 5 mg/m3
averaged over 8 hours or 10 mg/m3 averaged over 15 minutes (10 times the manufacturer's
suggested guideline), or
~ operations are performed in a confined space or in an area with limited ventilation. At least an
air purifying (organic vapor) respirator is required when:
~ the airborne concentrations of the HDI monomer exceed the TLV of 0.005 ppm, but are below
0.05 ppm (10 times the TLV), or
~ the airborne concentrations of the polyisocyanate (polymeric, oligomeric) exceed the
manufacturer's suggested guideline of 0.5 mg/m3 averaged over 8 hours, or 1.0 mg/m3 averaged
over 15 minutes but are below 10 mg/m3 (10 times the manufacturer's suggested guideline).
Ventilation Requirements:
Exhaust ventilation sufficient to keep the airborne concentrations of HDI and polyisocyanate
below their respective TLV and manufacturer's suggested guidelines must be utilized.
Exhaust air may need to be cleaned by scrubber or filters to reduce environmental
contamination.
Monitoring:
Refer to Patty's Industrial Hygiene and Toxicology- Volume 1 (3rd edition) Chapter 17 and
Volume III (1st edition) Chapter 3- for guidance concerning appropriate air sampling strategy to
determine airborne concentrations.
Medical Surveillance:
Medical supervision of all employees who handle or come in contact with HDI is recommended.
This should include preemployment and periodic medical examinations with respiratory function
tests (fev, fvc as a minimum). Persons with asthmatic-type conditions, chronic bronchitis, other
chronic respiratory diseases or recurrent skin eczema or sensitization should be excluded from
working with isocyanates. Once a person is diagnosed as being sensitized to isocyanates, no
further exposure can be permitted.
Additional Protective Measures:
Safety showers and eyewash stations should be available. Educate and train employees in safe
use of product. Follow all label information.
Section VIII - Reactivity Data
Stability ~~~~~~~~~~~~~~~~~~~~~ Stable under normal conditions.
Hazardous Polymerization:
May occur; contact with moisture or other materials which react with isocyanates or
temperatures over 400?F. (204?C) may cause polymerization.
Incompatibilities ~~~~~~~~~~~~~~~ Water, amines, strong bases, alcohols, metal compounds
and surface active materials.
Instability Conditions ~~~~~~~~~~~~ None Known.
Decomposition Products ~~~~~~~~~~ By heat and fires : carbon dioxide, oxides of nitrogen,
HCN, HDI.
U-111 Part B Page 7 of 10
Section IX - Spill and Leak Procedures
Spill or leak procedures:
Evacuate nonessential personnel. Remove all sources of ignition and ventilate the area.
Notify appropriate authorities if necessary. Put on personal protective equipment (see Section
VII). Dike or impound spilled material and control further spillage if feasible.
Cover the spill with sawdust, vermiculite, fuller's earth or other absorbent material. Pour
decontamination solution over spill area and allow to react for at least 10 minutes. Collect
material in open containers and add further amounts of decontamination solution. Remove
containers to a safe place, cover loosely, allow to stand for 24 to 48 hours. Wash down spill area
with decontamination solutions.
Decontamination Solutions:
Nonionic surfactant union carbide's Tergitol TMN-10 (20%) and water (80%); concentrated
ammonia (3-8%), detergent (2%) and water (90-95%).
Waste disposal method:
Waste must be disposed of in accordance with federal, state, and local environmental control
regulations. Incineration is the preferred method. Empty containers must be handled with care
due to product residue and flammable solvent vapor. Decontaminate containers prior to
disposal. Do not heat or cut empty container with electric or gas torch. (see Sections IV and
VIII).
Section X - Special Precautions and Storage Data
Storage Temperature (min/max)~~~~ -30?F. (-34?C)/122?F. (50?C)
Shelf Life ~~~~~~~~~~~~~~~~~~~~ One year, if unopened
Special Sensitivity:
If container is exposed to high heat, it can be pressurized and possibly rupture explosively.
HDI reacts slowly with water to form CO2 gas. This gas can cause sealed containers to expand
and possibly rupture explosively.
Handling/Storage Precautions:
Keep away from heat, sparks and open flame. Ground containers during storage and transfer
operations. Store in tightly closed containers to prevent moisture contamination. Do not reseal
if contamination is suspected. At maximum storage temperatures noted, material may slowly
polymerize without hazard. Ideal storage temperature range for ease of handling is 50-81?F.
(10-27?C.). Avoid contact with skin and eyes. Employee education and training in the safe use
and handling of this product are required under the OSHA Hazard Communication Standard.
Section XI - Shipping Information
D.O.T. Shipping Name ~~~~~~~~~~~~ Paint
Technical Shipping Name ~~~~~~~~~~ Polyisocyanate, Contains Xylene and Butyl Acetate
D.O.T. Hazard Class ~~~~~~~~~~~~~ Flammable Liquid
UN/NA Number ~~~~~~~~~~~~~~~~~UN1263
Product RQ (lbs.) ~~~~~~~~~~~~~~~~ 8000
D.O.T. Label ~~~~~~~~~~~~~~~~~~~~Flammable Liquid
D.O.T. Placard ~~~~~~~~~~~~~~~~~~ Flammable
Freight Class Bulk ~~~~~~~~~~~~~~~~Isocyanate
Freight Class Package ~~~~~~~~~~~~~Chemicals, NOI, NMFC 60000
U-111 Part B Page 8 of 10
Section XII - Animal Toxicity Data
Toxicity Data For: HDI homopolymer materials except where indicated.
Acute Toxicity
Oral LD50: Estimated to be greater than 10000 mg/kg (rats). (Based on the results of actual
tests conducted using specific HDI-homopolymer products).
Inhalation LC50: Lower respiratory (pulmonary) irritant. LC50 values ranging from 137-1150
mg/m3 were obtained in rats exposed to aerosols.
Eye effects: Severe irritant capable of inducing corneal injury (rabbit); maximum primary eye
irritation score: 54.6/110 for a 24 hour exposure.
Skin effects: Moderate irritant; primary dermal irritation score: 3.4/8.0 (rabbit).
Sensitization: Pulmonary and dermal sensitizer in animals and humans. Evidence exists that
cross-sensitization between HDI and other isocyanates, particularly hydrogenated MDI and TDI,
can occur.
Other Acute Effects: Ames Test: negative for 100% solids HDI homopolymer.
Subchronic Toxicity:
Rats exposed to an HDI homopolymer (biuret type), at 3.7, 17.5 and 76.6 mg/m3 for three weeks
(6 hours/day, 5 days/week) exhibited respiratory distress and inflamed areas of tissue in the
lungs and upper respiratory tract when exposed to 17.5 mg/m3 and above. The No Observable
Effect Level (NOEL) was 3.7 mg/m3. Rats exposed for three months (6 hours/day, 5 days/week)
to an HDI homopolymer (biuret type), at aerosol concentrations of 0.4, 3.4 and 21 mg/m3
exhibited lung weight increases at the highest dose. Histopathologic diagnosis of the test
animals revealed swelling and thickening in the lower respiratory tract as well as thickening of
the bronchio-alveolar areas of the lung and thickening of the septum in the 21 mg/m3 animals.
There were no effects noted in the upper and central respiratory tract.
The No Observable Effect Level (NOEL) in this study is considered to be 3.4 mg/m3.
Other Toxicity Data:
Mice were exposed to a liquid aerosol of an HDI homopolymer (isocyanate type), mixed with
acetone for three hours. The irritation potential expressed as the RD50 (the concentration which
is predicted to reduce the respiratory rate by 50%) was 20.8 mg/m3 (95% confidence interval =
18.3 to 23.9 mg/m3). Pulmonary (lung) irritation was observed first, followed by sensory (eye,
nose throat) irritation.
Toxicity Data For: Butyl Acetate
Acute Toxicity
Oral LD50 ~~~~~~~~~~~~~~~~~~~ 14000 mg/kg (rat)
Inhalation LC50 ~~~~~~~~~~~~~~~ 2000 ppm (rat)
Eye Effects ~~~~~~~~~~~~~~~~~~ Severe Irritation, 20 mg (rabbit)
Skin Effects ~~~~~~~~~~~~~~~~~~ Moderate Irritation, 500 mg/24h (rabbit)
Toxicity Data For: Xylene
Acute Toxicity
Oral LD50 ~~~~~~~~~~~~~~~~~~~ 4300 mg/kg (rat)
Dermal LD50 ~~~~~~~~~~~~~~~~~ Greater than 1700 mg/kg (rabbit)
Inhalation LC50 ~~~~~~~~~~~~~~~ 5000 ppm (rat, 4h exp)
Eye Effects ~~~~~~~~~~~~~~~~~~~Mild to Severe Irritation (rabbit)
Skin Effects ~~~~~~~~~~~~~~~~~~ Moderate Irritation (rabbit)
U-111 Part B Page 9 of 10
Section XIII - Federal Regulatory Information
OSHA Status~~~~~~~~~~~~~~~~~~~~This product is hazardous under the criteria of the
federal OSHA Hazard Communication Standard 29 CFR 1910.1200.
TSCA Status~~~~~~~~~~~~~~~~~~~~On TSCA Inventory
CERCLA Reportable Quantity:~~~~~~~xylene: 100 lbs.
~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~butyl acetate: 5000 lbs.
Sara Title III
Section 302 Extremely Hazardous Substances ~~~~ None
Section 311/312 Hazard Categories ~~~~~~~~~~~ Immediate Health Hazard
~~~~~~~~~~~ Delayed Health Hazard
~~~~~~~~~~~ Fire Hazard
~~~~~~~~~~~ Reactive Hazard
Section 313 Toxic Chemicals ~~~~~~~~~~~~~~~~ Xylene (CAS #1330-20-7) 12.5%
RCRA Status ~~~~~~~~~~~~~~~~~~~~~~~~~~~~When discarded in its purchased form, this
product meets the criteria of ignitability, and should be managed as a hazardous waste (EPA
hazardous waste number D001). (40 CFR 261.20-24)
Section XIV - Other Regulatory Information
The following chemicals are specifically listed by individual states; other product specific health
and safety data in other sections of the MSDS may also be applicable for state requirements. For
details on your regulatory requirements, you should contact the appropriate agency in your state.
Component Name
/CAS Number Concentration State Code
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Homopolymer of HDI 75% PA3, NJ4
28182-81-2
Xylene 12.5% PA1, MA, NJ1
1330-20-7
N-Butyl Acetate 12.5% PA1, MA, NJ1
123-86-4
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MA = Massachusetts Hazardous Substance List
NJ1 = New Jersey Hazardous Substance List
NJ4 = New Jersey Other - Included in Predominant Ingredients > 1%
PA1 = Pennsylvania Hazardous Substance List
PA3 = Pennsylvania Non-Hazardous Present at 3% or Greater
California Proposition 65
To the best of our knowledge, this product contains no levels of listed substances, which the state
of California has found to cause cancer, birth defects or other reproductive effects.
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U-111 Part B Page 10 of 10
Notice: This information is presented in good faith and believed to be accurate as of the
effective date below. However, no warranty is express or implied regarding the accuracy of this
data or the results to be obtained from the use thereof. Coatings For Industry, Inc. assumes no
responsibility for personal injury or property damage to vendees, users or third parties caused by
the material, such vendees or users assume all risks associated with the use of the material.
Regulatory requirements are subject to change and may differ from one location to another; it is
the buyer's responsibility to ensure that its activities comply with federal, state and local laws.
The preceding specific information is made for the purpose of complying with numerous federal,
state and local laws and regulations.
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