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MSDS Material Safety Data Sheet
CAS

75-09-2

File Name: 75-09.asp


Ashland Chemical Co. Date Prepared: 10/16/98

Date Printed: 06/21/99

MSDS No: 999.0018773-009.007I

METHYLENE CHLORIDE REAGENT ACS



__________________________________________________________________________



1. CHEMICAL PRODUCT AND COMPANY IDENTIFICATION



Material Identity

Product Name: METHYLENE CHLORIDE REAGENT ACS

General or Generic ID: CHLORINATED HYDROCARBON



Company Emergency Telephone Number:

Ashland Chemical Co. 1-800-ASHLAND (1-800-274-5263)

P.O. Box 2219 24 hours everyday

Columbus, OH 43216

614-790-3333 Regulatory Information Number:

1-800-325-3751



__________________________________________________________________________



2. COMPOSITION/INFORMATION ON INGREDIENTS



Ingredient(s) CAS Number % (by weight)

-------------------------------------------- ------------- -------------

METHYLENE CHLORIDE 75-09-2 100.0



__________________________________________________________________________



3. HAZARDS IDENTIFICATION



Potential Health Effects



Eye

Can cause eye irritation. Symptoms include stinging, tearing,

redness, and swelling of eyes.



Skin

Can cause skin irritation. Prolonged or repeated contact may dry

the skin. Symptoms may include redness, burning, and drying and

cracking of skin, burns and other skin damage. Passage of this

material into the body through the skin is possible, but it is

unlikely that this would result in harmful effects during safe

handling and use.



Swallowing

Swallowing small amounts of this material during normal handling

is not likely to cause harmful effects. Swallowing large amounts

may be harmful. This material can get into the lungs during

swallowing or vomiting. This results in lung inflammation and

other lung injury.



Inhalation

Breathing of vapor or mist is possible. Breathing this material

may be harmful. Symptoms usually occur at air concentrations

higher than the recommended exposure limits (See Section 8).



Symptoms of Exposure

Signs and symptoms of exposure to this material through breathing,

swallowing, and/or passage of the material through the skin may

include: stomach or intestinal upset (nausea, vomiting, diarrhea)

irritation (nose, throat, airways), central nervous system

depression (dizziness, drowsiness, weakness, fatigue, nausea,

headache, unconsciousness), central nervous system depression

(dizziness, drowsiness, weakness, fatigue, nausea, headache,

unconsciousness) and other central nervous system effects,

irregular heartbeat, elevated carbon monoxide levels in the blood,

and death.



Target Organ Effects

Overexposure to this material (or its components) has been

suggested as a cause of the following effects in laboratory

animals: kidney damage, liver damage.



Developmental Information

This material (or a component) has been shown to cause harm to the

fetus in laboratory animal studies. Harm to the fetus occurs only

at exposure levels that harm the pregnant animal. The relevance

of these findings to humans is uncertain.



Cancer Information

This material (or a component) causes cancer in laboratory animals

and therefore may present a carcinogenic risk to humans. This

material (or a component) is listed as a carcinogen by the

International Agency for Reseach on Cancer and the National

Toxicology Program.



Other Health Effects

No data



Primary Route(s) of Entry

Inhalation, Skin absorption, Skin contact, Eye contact.



__________________________________________________________________________



4. FIRST AID MEASURES



Eyes

If symptoms develop, immediately move individual away from

exposure and into fresh air. Flush eyes gently with water for at

least 15 minutes while holding eyelids apart; seek immediate

medical attention.



Skin

Remove contaminated clothing. Flush exposed area with large

amounts of water. If skin is damaged, seek immediate medical

attention. If skin is not damaged and symptoms persist, seek

medical attention. Launder clothing before reuse.



Swallowing

Seek medical attention. If individual is drowsy or unconscious,

do not give anything by mouth; place individual on the left side

with the head down. Contact a physician, medical facility, or

poison control center for advice about whether to induce vomiting.

If possible, do not leave individual unattended.



Inhalation

If symptoms develop, immediately move individual away from

exposure and into fresh air. Seek immediate medical attention;

keep person warm and quiet. If person is not breathing, begin

artificial respiration. If breathing is difficult, administer

oxygen.



Note to Physicians

Inhalation of high concentrations of this material, as could occur

in enclosed spaces or during deliberate abuse, may be associated

with cardiac arrhythmias. Sympathomimetic drugs may initiate

cardiac arrhythmias in persons exposed to this material. This

material is an aspiration hazard. Potential danger from

aspiration must be weighed against possible oral toxicity (See

Section 3 - Swallowing) when deciding whether to induce vomiting.

Preexisting disorders of the following organs (or organ systems)

may be aggravated by exposure to this material: skin, lung (for

example, asthma-like conditions), liver, kidney, Exposure to this

material may aggravate any preexisting condition sensitive to a

decrease in available oxygen, such as chronic lung disease,

coronary artery disease or anemias. Individuals with preexisting

heart disorders may be more susceptible to arrhythmias (irregular

heartbeats) if exposed to high concentrations of this material.



__________________________________________________________________________



5. FIRE FIGHTING MEASURES



Flash Point

Not applicable



Explosive Limit

Not applicable



Autoignition Temperature

No data



Hazardous Products of Combustion

May form: carbon dioxide and carbon monoxide, chlorine, hydrogen

chloride, phosgene.



Fire and Explosion Hazards

No flash to boiling point. This product contains halogenated

solvents which inhibit flashing until the halogenated solvent has

been evaporated away. The product may become combustible or

flammable after this occurs. Vapors are heavier than air and may

travel along the ground or may be moved by ventilation and ignited

by pilot lights, other flames, sparks, heaters, smoking, electric

motors, static discharge, or other ignition sources at locations

distant from material handling point.



Extinguishing Media

water fog, carbon dioxide, dry chemical.



Fire Fighting Instructions

Wear a self-contained breathing apparatus with a full facepiece

operated in the positive pressure demand mode with appropriate

turn-out gear and chemical resistant personal protective

equipment. Refer to the personal protective equipment section of

this MSDS.



NFPA Rating

Health - 2, Flammability - 1, Reactivity - 0



__________________________________________________________________________



6. ACCIDENTAL RELEASE MEASURES



Small Spill

Absorb liquid on vermiculite, floor absorbent or other absorbent

material. Persons not wearing proper personal protective

equipment should be excluded from area of spill.



Large Spill

Prevent run-off to sewers, streams or other bodies of water. If

run-off occurs, notify proper authorities as required, that a

spill has occurred. Persons not wearing protective equipment

should be excluded from area of spill until clean-up has been

completed. Stop spill at source, dike area of spill to prevent

spreading, pump liquid to salvage tank. Remaining liquid may be

taken up on sand, clay, earth, floor absorbent, or other absorbent

material and shoveled into containers.



__________________________________________________________________________



7. HANDLING AND STORAGE



Handling

Containers of this material may be hazardous when emptied. Since

emptied containers retain product residues (vapor, liquid, and/or

solid), all hazard precautions given in the data sheet must be

observed.



Storage

Aluminum equipment should not be used for storage and/or transfer,

e.g. pumps, mixers, fittings, storage tanks, etc. Contact with

aluminum parts in a pressurizable fluid system may cause violent

reactions.



__________________________________________________________________________



8. EXPOSURE CONTROLS/PERSONAL PROTECTION



Eye Protection

Chemical splash goggles in compliance with OSHA regulations are

advised; however, OSHA regulations also permit other type safety

glasses. Consult your safety representative.



Skin Protection

Wear resistant gloves (consult your safety equipment supplier).,

To prevent skin contact, wear impervious clothing and boots..



Respiratory Protections

If workplace exposure limit(s) of product or any component is

exceeded (see exposure guidelines), a NIOSH/MSHA approved air

supplied respirator is advised in absence of proper environmental

control. OSHA regulations also permit other NIOSH/MSHA

respirators (negative pressure type) under specified conditions

(see your industrial hygienist). Engineering or administrative

controls should be implemented to reduce exposure. See 29 CFR

1910.1052 for specific OSHA requirements for employee exposure to

methylene chloride.



Engineering Controls

Provide sufficient mechanical (general and/or local exhaust)

ventilation to maintain exposure below TLV(s).



Exposure Guidelines

Component

----------



METHYLENE CHLORIDE (75-09-2)

OSHA VPEL 25.000 ppm - TWA See 29 CFR 1910.1052

OSHA VPEL 125.000 ppm - STEL (as determined over a sampling period of

fifteen minutes)

ACGIH TLV 50.000 ppm - TWA



__________________________________________________________________________



9. PHYSICAL AND CHEMICAL PROPERTIES



Boiling Point

(for product) 104.0 F (40.0 C) @ 760 mmHg



Vapor Pressure

(for product) 340.000 mmHg @ 68.00 F



Specific Vapor Density

2.930 @ AIR=1



Specific Gravity

1.318 @ 77.00 F



Liquid Density

10.970 lbs/gal @ 77.00 F

1.318 kg/l @ 25.00 C



Percent Volatiles

100.0 %



Volatile Organic Compounds (VOC)

> 999.000 g/l

10.970 lbs/gal



Evaporation Rate

1.80 (ETHER)



Appearance

No data



State

LIQUID



Physical Form

HOMOGENEOUS SOLUTION



Color

CLEAR, APHA COLOR 10 MAX



Odor

No data



pH

Not applicable



Bulk Density

1.470 lbs/ft3



__________________________________________________________________________



10. STABILITY AND REACTIVITY



Hazardous Polymerization

Product will not undergo hazardous polymerization.



Hazardous Decomposition

May form: carbon dioxide and carbon monoxide, chlorine, hydrogen

chloride, phosgene, Open flame, welding arcs, resistance heaters,

etc., which can result in thermal decomposition releasing hydrogen

chloride and small amounts of phosgene and chlorine..



Chemical Stability

Stable. Gross contamination with water can cause hydrolysis,

producing small amounts of hydrochloric acid.



Incompatibility

Avoid contact with: amines, reactive metals such as aluminum and

magnesium, strong alkalies, strong oxidizing agents.



__________________________________________________________________________



11. TOXICOLOGICAL INFORMATION



No data



__________________________________________________________________________



12. ECOLOGICAL INFORMATION



No data



__________________________________________________________________________



13. DISPOSAL CONSIDERATION



Waste Management Information

Dispose of in accordance with all applicable local, state and

federal regulations.



__________________________________________________________________________



14. TRANSPORT INFORMATION



DOT Information - 49 CFR 172.101

DOT Description:

DICHLOROMETHANE MIXTURE,6.1,UN1593,III



Container/Mode:

55 GAL DRUM/TRUCK PACKAGE



NOS Component:

None



RQ (Reportable Quantity) - 49 CFR 172.101

Product Quantity (lbs) Component

---------------------- --------------------------------------------------

1000 DICHLOROMETHANE



__________________________________________________________________________



15. REGULATORY INFORMATION



US Federal Regulations

TSCA (Toxic Substances Control Act) Status

TSCA (UNITED STATES) The intentional ingredients of this

product are listed.



CERCLA RQ - 40 CFR 302.4(a)

Component RQ (lbs)

---------------------------------------- ---------

METHYLENE CHLORIDE 1000



SARA 302 Components - 40 CFR 355 Appendix A

None



Section 311/312 Hazard Class - 40 CFR 370.2

Immediate(X) Delayed(X) Fire( ) Reactive( ) Sudden

Release of Pressure( )



SARA 313 Components - 40 CFR 372.65

Section 313 Component(s) CAS Number %

---------------------------------------- ------------- ------

DICHLOROMETHANE (METHYLENE CHLORIDE) 75-09-2 100.00



International Regulations

Inventory Status

Not determined



State and Local Regulations

California Proposition 65

The following statement is made in order to comply with the

California Safe Drinking Water and Toxic Enforcement Act of

1986: This product contains the following substance(s) known to

the state of California to cause cancer.

DICHLOROMETHANE (METHYLENE CHLORIDE)



New Jersey RTK Label Information

METHYLENE CHLORIDE 75-09-2



Pennsylvania RTK Label Information

METHANE, DICHLORO- 75-09-2



__________________________________________________________________________



16. OTHER INFORMATION



The information accumulated herein is believed to be accurate but

is not warranted to be whether originating with the company or

not. Recipients are advised to confirm in advance of need that the

information is current, applicable, and suitable to their

circumstances.


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